黄苏婷,杭方学,韦春波,谢彩锋,李凯

• 1:广西大学轻工与食品工程学院
• 2:广西凤糖生化股份有限公司

摘要(Abstract)：

利用固相微萃取方法(SPME)提取红糖中的挥发性香气成分,从样品浓度、样品添加量、NaCl添加量、萃取温度和萃取时间5个方面进行优化,确定最终的萃取参数为:样品浓度60%,样品添加量6.00g,NaCl添加量0.60g,萃取时间50min,萃取温度50℃。在此基础上对自制红糖以及古方和太古2种市售红糖进行气相色谱-质谱(GC-MS)检测,分析红糖的挥发性香气成分,确定其组成与相对含量,初步判定其中乙醛、2-甲基丁醛、3-甲基丁醛、2,6-二甲基吡嗪、壬醛、2,6-二乙基-吡嗪、2,3,5-三甲基吡嗪、糠醛、2,3-二甲基吡嗪、癸醛和2-乙酰基吡咯是主要的挥发性香气成分。

关键词(KeyWords)： 红糖;挥发性;香气物质;固相微萃取;气相色谱-质谱

Abstract:

Keywords:

基金项目(Foundation): 广西科技计划项目(桂科AA17204092,桂科AB16380011);; 南宁市科技计划项目(20161021)

作者(Author): 黄苏婷,杭方学,韦春波,谢彩锋,李凯

参考文献(References)：

• [1]JafféW R.Health effects of non-centrifugal sugar(NCS):a review[J].Sugar Tech,2012,14(2):87-94.
• [2]Guerra M J,Mujica M V.Physical and chemical properties of granulated cane sugar"panelas"[J].Ciência E Tecnologia De Alimentos,2010,30(1):250-257.
• [3]Takara K, Kinjyo A, Matsui D,et al. Antioxidative phenolic compounds from non-sugar fraction in Kokuto,non-centrifugal cane sugar[J].Nippon Nogeikagaku Kaishi,2000,74(8):885-890.
• [4]Calabia B P,Tokiwa Y.Production of D-lactic acid from sugarcane molasses,sugarcane juice and sugar beet juice by Lactobacillus delbrueckii[J].Biotechnology Letters,2007,29(9):1329-1332.
• [5]Harish N M A,Sathisha U V,Manohar M P,et al.Cytoprotective and antioxidant activity studies of jaggery sugar[J].Food Chemistry,2009,115(1):113-118.
• [6]Bao G Y,Lan Y H,Zhu S X.The active nutrients and application development advantages of brown sugar[J].Sugarcane &Canesugar,2015(11):239-241.
• [7]Brown L O.Studies on the turbidity of cane juice and raw sugar[J].Journal of Food Process Engineering,2008(14):77-80.
• [8]Inafuku M,Toda T,Okabe T,et al.Effect of Kokuto,a non-centrifugal cane sugar,on the development of experimental atherosclerosis in Japanese quail and apolipoprotein E deficient mice[J].Food Science &Technology International Tokyo,2007,13(1):61-66.
• [9]Asikin Y,Hirose N,Tamaki H,et al.Effects of different drying-solidification processes on physical properties,volatile fraction,and antioxidant activity of non-centrifugal cane brown sugar[J].LWT-Food Science and Technology,2016,66:340-347.
• [10]Asikin Y,Kamiya A,Mizu M,et al.Changes in the physicochemical characteristics,including flavour components and Maillard reaction products,of non-centrifugal cane brown sugar during storage[J].Food Chemistry,2014,149(8):170-177.
• [11]吴光忠,何炯灵,黄炳文,等.果香型米醋的研制及风味分析[J].中国调味品,2018,43(9):121-125.
• [12]Romeo V,Ziino M,Giuffrida D,et al.Flavour profile of capers(Capparis spinosa L.)from the Eolian Archipelago by HS-SPME/GC-MS[J].Food Chemistry,2007,101(3):1272-1278.
• [13]姜文广,李记明,徐岩,等.4种酿酒红葡萄果实的挥发性香气成分分析[J].食品科学,2011,32(6):225-229.
• [14]杨雅瑜,刘玉德,张媛,等.正交实验优化多频超声波辅助法提取绿茶茶多酚工艺[J].食品工业科技,2014,35(19):189-193.