食品防腐剂的检测新技术进展New technologies for the detection of food preservative
严蓓蓓,孙芸,熊晓辉
摘要(Abstract):
食品中防腐剂的定性定量检测越来越受到关注。文章综述了食品中防腐剂定性定量检测方面的研究进展,详细介绍了几种新的预处理技术(包括固相萃取、固相微萃取、亚临界水萃取等)以及新的检测技术(包括液相色谱-质谱联用、红外光谱、毛细管胶束电动色谱、微乳液毛细管电动色谱、生物传感器等),为食品中防腐剂的便捷、准确检验提供参考。
关键词(KeyWords): 食品安全;防腐剂;预处理;检测
基金项目(Foundation):
作者(Author): 严蓓蓓,孙芸,熊晓辉
参考文献(References):
- [1]陈发河,吴光斌,林华玲,等.固相萃取-反相高效液相色谱法同时测定多种食品添加剂[J].食品学报,2006,6(6):126-132.
- [2]Gonzalez M,Gallego M,Valcartel M.Si multaneousgaschromatogrphic determinationof food preservativesfollowing solid-phaseextraction[J].Journal of Chro-matography A,1998,823:321-329.
- [3]Gonzalez M,Gallego M,Valcarcel M.Gas chromato-graphic flow method for the preconcentration and si-multaneous determination of antioxidant and preserva-tive additives infattyfoods[J].Journal of Chroma-tography A,1999,848:529-536.
- [4]刘杨岷,王利平,袁身淑.周相微萃取快速测定酱油中的对羟基苯甲酸乙酯[J].中国调味品,2005(9):53-56.
- [5]Chunzhou Dong,Yong Mei,Lin Chen.Si multaneousdetermination of sorbic and benzoic acids in fooddressing by headspacesolid-phase microextractionandgaschromatography[J].Journal of ChromatographyA,2006,1117:109-114.
- [6]Chunzhou Dong,Wenfang Wang.Headspace solid-phase microextraction applied to the si multaneousdetermination of sorbic and benzoic acids in beverages[J].Analytica Chi mica Acta,2006(562):23-29.
- [7]王耀,陆晓华.亚临界水萃取肉制品中的亚硝酸盐的研究[J].食品工业科技,2006,12:178-180.
- [8]许秀敏,吴西梅,梁春穗,等.液相色谱-质谱联用检测食品中苯甲酸、山梨酸、糖精钠[J].中国卫生检验杂志,2005,9(15):1057-1059.
- [9]Yukiko Abe-Onishi,Chikako Yomota,Naoki Sugi moto,et al.Determination of benzoyl peroxide and benzoicacidin wheatflour by high-performanceliquidchroma-tography and its identification by high-performanceliquid chromatography-mass pectrometry[J].Journalof Chromatography A,2004,1040:209-214.
- [10]倪昕路,褚庆华,郭德华.傅里叶变换红外光谱和高效液相色谱在食品添加剂分析中的配合运用[J].检验检疫科学,1999,1(9):12-13.
- [11]回瑞华,侯冬岩,关崇新,等.红外光谱法测定奶粉中苯甲酸钠的含量[J].食品科学,2003(8):121-123.
- [12]Mary C,Boyce.Si multaneous determination of antiox-idants,preservatives and sweeteners permitted asadditives in food by mixed micellar electrokineticchromatography[J].Journal of Chromatography A,1999,847:369-375.
- [13]Richard AFrazier,Elizabeth LInns,Nieolo Dossi.Development of a capillary electrophoresis methodfor thesi multaneous analysis of artificial sweeteners,preservatives and colours in soft drinks[J].Joumalof Chromatography A,2000(876):213-220.
- [14]Hsi Yahuang,Chia Lingchuang,Chen Wenchiu.Application of microemulsion electrokinetic chroma-tography for the detection of preservatives in foods[J].Food Chemistry,2005(89):315-322.
- [15]Mahuzier P E,Altria KD,Clark BJ.Selective andquantitative analysis of 4-hydroxybenzoate preser-vatives by microemulsion electrokinetic chromatogra-phy[J].J Chromatogr A,2001,924:465-470.
- [16]MinZhao,Brynn Hibbert D,Justin GoodingJ.Deter-mination of sulfite in beer samples using an ampe-rometricfill and flow channel biosensor employingsulfite oxidase[J].Analytica Chi mica Acta,2006,556:195-200.
- [17]Mustafa Kemal Sezginturk,Erhan Dinc,kaya.Direct determination of sulfite in food samples by abiosensor based on plant tissue homogenate[J].Talanta,2005,65:998-1002.
- [18]Erhan Dincaya,Mustafa Kemal Sezginturk,ErolAkyil maz.Sulfite determination usingsulfite oxidasebiosensor based glassy carbon electrode coated withthin mercuryfli m[J].Food Chemistry,2007,101:1540-1544.
- [19]Serge Da Silva,Serge Cosnier,Gabriela Al meida M,et al.An efficient poly(pyrrole-viologen)-nitrite-reductase biosensor for the mediated detection ofnitrite[J].Electrochemistry Communications,2 0 0 4(6):404-408.
- [20]Morales MD,Morante S,Escarpa A.Design of acomposite amperomerric enzyme electrode for thecontrol of the benzoic acid content in food[J].Talanta,2002,57:1189-1198.