芽菜发酵过程中挥发性香气成分的研究Annlysis of Volatile Flavor Compounds in the Process of Yacai Fermentationed
吴华昌,张良,邓静,李萍萍,肖辰,沈芳
摘要(Abstract):
采用顶空固相微萃取对不同发酵时间芽菜的挥发性香气组分进行萃取,再经气质联用进行分析鉴定,共鉴定出75个挥发组分。其中,新鲜芽菜含有挥发性香味成分29种,新腌制含有22种,腌制40天含有21种,腌制80天含有22种,腌制120天含有22种,腌制160天含有27种。挥发性的醇类、酸类、酯类和烷烃类等化合物构成了芽菜的主体香味物质。
关键词(KeyWords): 芽菜;顶空-固相微萃取;气质联用仪;挥发性成分
基金项目(Foundation): 四川省科技厅应用基础项目(2010JY0081)
作者(Author): 吴华昌,张良,邓静,李萍萍,肖辰,沈芳
参考文献(References):
- [1]Wu Z,Lee Y Y.Inhibition of the enzymatic hydrolysis ofthe cellulose by ethanol[J].Biotechnology letters,1997,19:977-979.
- [2]Montesinos T,Navarro J.Production of Alcohol from RawWheat Flour by Amyloglucosidase and Saccharomyces cere-visiae[J].Enzyme Microb Technol,2000,27(3):362-370.
- [3]Jeyaram K.Bacterial species associated with traditionalstarter cultures used for fermented bamboo shoot productionin Manipur state of India[J].International Journal of FoodMicrobiology,2010,143(1-2):1-8.
- [4]Nancy J.Selection and characterization of mixed starter cul-tures for lactic acid fermentation of carrot,cabbage,beetand onion vegetable mixtures[J].International Journal ofFood Microbiology,2001,64(3):261-275.
- [5]赵新淮.食品化学[M].北京:化学工业出版社,2006:26.
- [6]Prososki R A M.Solvent Type Affects the Number,Distri-bution,and Relative Quantities of Volatile CompoundsFound in Sweety Whey Powder[J].Journal of Dairy Sci-ence,2007,90(2):523-531.
- [7]Mahajan S S.Aroma Compounds in Sweety Whey Powder[J].Journal of Dairy Science,2004,87(12):4057-4063.
- [8]Xie J C.Aromatic Constituents from Chinese TraditionalSmoke-cured Bacon of Mini-pig[J].Food Science andTechnology International,2008,14(4):329-340.
- [9]Yahya F.Supercritical carbon dioxide and solvent extractionof 2-acetyl-1-pyrroline from Pandan leaf:The effect of pre-treatment[J].Journal of Supercritical Fluids,2010,55(1):200-207.
- [10]Da Porto.Countercurrent supercritical fluid extraction ofgrape-spirit[J].Journal of Supercritical Fluids,2010,55(1):128-131.
- [11]Kamatou G P P.Head-space volatiles of Gethyllis afraand G.ciliaris fruits(“kukumakranka”)[J].South Afri-can Journal of Botany,2008,74(4):768-770.
- [12]Tomoko Maeda,Ji Kim,Yoshihito Ubukata.Analysis ofvolatile compounds in Polished-graded wheat flours usingheadspace sorptive extraction[J].European Food Re-search and Technology.A,2008,227(4):1233-1241.
- [13]Canuti V,Conversano M,Calzi ML,et al.Headspace sol-id-phase microextraction-gas chromatography-massspectrometry for profiling free volatile compounds inCabernet Sauvignon grapes and wines[J].Journal of Chro-matography.A,2009,1216(15):3012-3022.
- [14]Benincasa C,DeNino A,Lombardo N,et al.Assay of a-roma active components of virgin olive oils from southernItalian regions by SPME-GC/Ion Trap Mass Spectrometry[J].Journal of Agricultural and Food Chemistry,2005,51(12):733-741.
- [15]Liu Y H.Contents of various types of proteins and watersoluble peptides in sufu during ageing and the amino acidcomposition of taste oligopeptides[J].Journal of the Chi-nese Agricultural and Chemical Society,1994,32(6):276-283.
- [16]Nogueira MCL,Lubachevsky G,Rankin SA.A study ofthe volatile composition of Minas cheese[J].LebensmWissu Technology,2005,38(3):555-563.
- [17]Izco J M,Torre P.Characterisation of volatile flavourcompounds in Roncal cheese extracted by the‘purge andtrap’method and analysed by GC-MS[J].Food Chemistry2000,70(5):409-417.
- [18]林丽钦.十字花科植物的风味物质及其降解化学[J].福建轻纺,1999,119(4):1-5.
- [19]刘明春.榨菜加工过程中挥发性物质的形成及变化的研究[D].重庆大学,2009:34-38.
- [20]Fernandez-Garcia E,Carbonell M,Gaya P,et al.Evolu-tion of the volatile components of ewes raw milk Zamoranocheese.Seasonal variation[J].International Dairy Jour-nal,2004,14:701-711.