超声提取葡萄籽原花青素工艺的优化及其抗氧化活性研究Study on Optimization of Ultrasonic Extraction of Procyanidins from Grape Seeds and Its Antioxidant Activity
金华,刘志刚,曾晓丹,高艳,马明硕
摘要(Abstract):
研究利用响应曲面法优化超声提取葡萄籽原花青素的工艺。在单因素实验基础上,采用中心组合设计响应面实验,考察了提取温度、液料比、乙醇浓度以及超声时间对原花青素提取率的影响,并建立回归模型。优化后的工艺:提取温度55℃,液料比20(mL/g),乙醇浓度65%,超声时间10min;在此条件下葡萄籽原花青素的提取率为2.482%,与回归模型预测值的相对偏差为0.36%。同时进行了提取物的抗氧化性检验,结果表明葡萄籽原花青素对超氧阴离子自由基具有较好的清除能力,且呈剂量相关性。
关键词(KeyWords): 葡萄籽原花青素(GPA);超声提取;响应曲面;抗氧化
基金项目(Foundation): 吉林化工学院科学技术研究项目(吉化院合字[2012]第049号)
作者(Author): 金华,刘志刚,曾晓丹,高艳,马明硕
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