动态夹带剂强化超临界CO2萃取万寿菊中叶黄素Supercritical carbon dioxide extraction of lutein ester from marigold(Tagetes erect L.)with continuous co-solvent
王琦,高彦祥,刘璇
摘要(Abstract):
以粉碎后的万寿菊花为原料,研究了不同萃取压力、温度、夹带剂浓度和夹带剂种类对超临界二氧化碳萃取叶黄素的影响。结果表明,叶黄素萃取率随压力、温度和夹带剂浓度的升高先升高后降低;以MCT作为夹带剂,叶黄素的提取率高于以大豆油、葵花籽油、菜籽油和正己烷作为夹带剂。
关键词(KeyWords): 夹带剂;超临界CO_2萃取;叶黄素
基金项目(Foundation):
作者(Author): 王琦,高彦祥,刘璇
参考文献(References):
- [1]惠伯棣.类胡萝卜素化学及生物化学[M].北京:中国轻工业出版社,2005.1.
- [2]廖萍泰,惠伯棣,裴凌鹏,等.叶黄素的体外抗氧化功能[J].食品与发酵工业,2005,31(4):46-49.
- [3]Kiokias S,Oreopoulou V.Antioxi dant properties of natural carotenoid extracts against the AAPH-ini-tiated oxidation of food emulsions[J].Innovative Food Science and Emerging Technologies7(2006)132-139.
- [4]Nishino.H,Tokude.H,Murakoshi.M,Satomi.Y,Masuda.M,Onozuka.M,Yamaguchi.S,Tak-ayasu.J,Tsuruta.J,Okuda.M,Khachik.F,Narisawa.T,Takasuka.N,Yanom.M,Cancer pre-vention by natural carotenoid[J].BioFactors,2000(13):89-94.
- [5]Sowbhagya.H.B,Sampathu.S.R,Krishnamur-thy.N,Natural Colorant from Marigold-Chemistry and Technology[J].Food reviews international,2004(12):33-50.
- [6]Wenzel.A.J,Sheehan.J.P,Burke.J.D,Lefsrud.M.G,Curran-Celentano.J,Dietaryintake and serum concentrations of lutein and zeaxanthin,but not macular pigment optical density,are related in spouses[J].Nutrition Research,2007(27):462-469.
- [7]Liu.B,et al.Extraction of berberine from rhizome of Coptis chinensis Franch using supercritical fluid ex-traction[J].Journal of Pharmaceutical and Biomed-ical Anaysis,2006(41):1056-1060.
- [8]Casas.L,et al.Effect of the addition of cosolvent on the supercritical fluid extraction of bioactive com-pounds from Helianthus annulus L[J].Supercritical Fluids,2007(41):43-49.
- [9]陈俊英,曹文豪,罗娜,等.不同夹带剂条件下超临界萃取薯蓣皂素的研究[J].河南工业大学学报,2006,27(1):60-63.
- [10]藏志清,周端美,林述英.超临界二氧化碳萃取红辣椒的夹带剂筛选[J].农业工程学报,1999,15(2):208-213.
- [11]Sun.M,Temelli.F,Supercritical carbon dioxide extraction of carotenoids fromcarrot using canola oil as a continuous co-solvent[J].Journal of Supercr-itical Fluids.2006(37):397-408.
- [12]Vasapollo.G,et al.Innovativesupercritical CO2ex-traction of lycopene fromtomato in the presence of vegetable oil as co-solvent[J].Thejournal of Sup-ercritical fluids,2004(29):87-96.
- [13]马清香,徐响,高彦祥.超I临界CO萃取万寿菊花中叶黄素的研究[J].农业工程学报.2007,23(8):257-260.
- [14]魏林.小麦粉水分测定方法的比较[J].山地农业生物学报,2005,24(4):363-365.
- [15]FAO/WHO press.Compendium of food additive specifications[M].USA:1990,52(9):105-106.
- [16]Krichnavaruk,S.Supercriticalcarbondioxideextraction ofastaxanthinfrom...[J].Bioresour.Technol.2007,doi:10.1016/j.biortech.2007.10.049.
- [17]Bamberger T,Erickoson J C,Cooney C L.Measurement and model prediction of solubilities of purefatty acids,puretriglycerides,and mixtures of triglycerides in supercritical carbon dioxide[J].J.Chem.Eng,Data,1988,33:327-333.
- [18]Gil-stnda犂,F.Temelli,Solubility behavior of ternarysystems oflipids,cosolventsandsupercritical carbon dioxide and processing aspects[J].J.Su-percrit.Fluid,2005,36:1-15.
- [19]Nodar,D.Characterisation and process developm-ent of supercritical fluid extraction of soybean oil[J].Food Science and Technology International.2002,8(6):337-342.
- [20]Roy,B.C.Effect of temperature and pressure on the extraction yield of oil from sunflower seed withsupercriticalcarbondioxide[J].Journalof Applied Sciences,2006,6(1):71-75.