不同地区典型火腿的脂肪酸组成和挥发性风味物质对比分析Comparative Analysis of Fatty Acid Composition and Volatile Flavor Substances of Typical Ham from Different Regions
徐恒,王晓雨,裴龙英,刘伟,张恒,王金铎,耿瑞娟,马志凯,陈蕙兰
摘要(Abstract):
为比较不同地区典型干腌火腿的脂肪酸和挥发性风味物质组成,以5种火腿(金华火腿、宣威火腿、如皋火腿、光控低盐火腿和伊比利亚火腿)为原料,对其脂肪酸含量和挥发性风味物质进行了对比分析。结果表明,5种火腿中,光控低盐火腿的脂肪酸总含量最高,如皋火腿的脂肪酸总含量最低。棕榈酸、硬脂酸、油酸和亚油酸是5种火腿中4种主要的游离脂肪酸,其中光控低盐火腿的棕榈酸、硬脂酸和油酸含量均显著高于其余4种火腿(P<0.05),与金华火腿和宣威火腿的亚油酸含量差异不显著(P>0.05)。采用SPME-GC-MS方法对火腿的风味物质进行定量分析,从5种火腿中共检测出72种挥发性风味物质。醛类、醇类、酯类和酸类是5种火腿中的主要风味物质,其中醛类物质是5种火腿中种类最多、含量最丰富的组分,以金华火腿的挥发性风味物质种类最多。该研究结果可初步评价不同地区火腿的脂质和风味特性,为改善火腿加工工艺、提高品质及构建火腿风味特性标准化提供了一定的理论依据。
关键词(KeyWords): 火腿;脂肪酸组分;挥发性风味物质;对比分析
基金项目(Foundation): 新疆维吾尔自治区重点研发计划项目(2020B02011);; 新疆理工学院校级科研项目(ZT202101)
作者(Author): 徐恒,王晓雨,裴龙英,刘伟,张恒,王金铎,耿瑞娟,马志凯,陈蕙兰
参考文献(References):
- [1]ZHOU C Y,ZHAN G,PAN D D,et al.Charactering the spoilage mechanism of “three sticks” of Jinhua ham[J].Food Science and Human Wellness,2022,11(5):1322-1330.
- [2]SHI Y N,LI X,HUANG A X.Multivariate analysis approach for assessing coated dry-cured ham flavor quality during long-term storage[J].Journal of Food Science and Technology,2021,58(2):651-659.
- [3]邢路娟,郝月静,左庆翔,等.金华火腿中生物活性肽的血管紧张素转化酶调节功能及其分离纯化[J].中国食品学报,2023,23(5):78-86.
- [4]LI F Y,FENG X,ZHANG D N,et al.Physical properties,compositions and volatile proffles of Chinese dry-cured hams from different regions[J].Journal of Food Measurement and Characterization,2020,14(1):492-504.
- [5]LIU S Y,WANG G Y,XIAO Z C,et al.1H-NMR-based water-soluble low molecular weight compound characterization and free fatty acid composition of five kinds of Yunnan dry-cured hams[J].LWT-Food Science and Technology,2019,108(6):174-182.
- [6]LIU D Y,BAI L,FENG X,et al.Characterization of Jinhua ham aroma profiles in specific to aging time by gas chromatography-ion mobility spectrometry (GC-IMS)[J].Meat Science,2020,168:108178.
- [7]WANG W L,FENG X,ZHANG D N,et al.Analysis of volatile compounds in Chinese dry-cured hams by comprehensive two-dimensional gas chromatography with high-resolution time-of-flight mass spectrometry[J].Meat Science,2018,140(14):14-25.
- [8]梁定年,薛桥丽,黄启超,等.三川焐灰火腿和风干火腿发酵过程中理化性质变化[J].肉类研究,2019,33(9):19-24.
- [9]HUAN Y J,ZHOU G H,ZHAO G M,et al.Changes in flavor compounds of dry-cured Chinese Jinhua ham during processing[J].Meat Science,2005,71(2):291-299.
- [10]施忠芬,王桂瑛,陈红艳,等.GC-MS法测定宣威火腿中脂肪酸组成[J].食品与发酵工业,2012,38(9):141-145.
- [11]ZHAO Y,HE W Y,ZHAN P,et al.A comprehensive analysis of aroma quality and perception mechanism in ginger-infused stewed beef using instrumental analysis,sensory evaluation and molecular docking[J].Food Chemistry,2024,460:140435.
- [12]李玲,张敬竟,王桂瑛,等.宣威火腿与金华火腿中游离脂肪酸组成比较分析[J].食品工业科技,2019,40(15):225-229,234.
- [13]刘姝韵,王桂瑛,谷大海,等.五种云南火腿游离脂肪酸含量比较分析[J].食品与发酵工业,2019,45(2):207-213.
- [14]张婷,王振宇,李铮,等.饲喂大麦对大河乌猪干腌火腿理化特性及脂肪酸组成的影响[J].中国农业科学,2016,49(2):331-338.
- [15]黄晶晶,周迎芹,张福生,等.6种安徽地方火腿不同部位特征香气的气相色谱-离子迁移谱表征[J].肉类研究,2021,35(8):28-36.
- [16]CARRAPISO A I,NOSEDA B,GARCIA C,et al.SIFT-MS analysis of Iberian hams from pigs reared under different conditions[J].Meat Science,2015,104:8-13.
- [17]LORENZO J M,CARBALLO J,FRANCO D.Effect of the inclusion of chestnut in the finishing diet on volatile compounds of dry-cured ham from Celta pig breed[J].Meat Science,2013,12(11):2002-2012.
- [18]GARCIA-GONZALEZ D L,RONCALES P,CILLA I,et al.Interlaboratory evaluation of dry-cured hams (from France and Spain) by assessors from two different nationalities[J].Meat Science,2006,73(3):521-528.
- [19]GARCIA C,BERDAGUE J,ANTEQUERA T,et al.Volatile components of dry cured Iberian ham[J].Food Chemistry,1991,41(1):23-32.
- [20]ZHU C Z,TIAN W,LI M Y,et al.Separation and identification of peptides from dry-cured Jinhua ham[J].International Journal of Food Properties,2018,20(3):2980-2989.
- [21]SALAZAR E,TEJADA L.Fatty acids and free amino acids changes during processing of a Mediterranean native pig breed dry-cured ham[J].Foods,2020,9(9):1170.
- [22]SWANSON D,BLOCK R,MOUSA S A.Omega-3 fatty acids EPA and DHA,health benefits throughout life[J].Advances in Nutrition,2012,3(1):1-7.
- [23]王丽,刘光宪,张德权,等.安福火腿游离脂肪酸、风味物质及氨基酸分析[J].食品工业科技,2021,42(16):236-242.
- [24]ZHANG Y Y,WU H Z,TANG J,et al.Influence of partial replacement of NaCl with KCl on formation of volatile compounds in Jinhua ham during processing[J].Food Science and Biotechnology,2016,25(2):379-391.
- [25]王勇勤,郭新,黄笠原,等.基于电子鼻和气相色谱-质谱联用技术分析不同贮藏时间羊肉火腿香气成分[J].食品科学,2019,40(2):215-221.
- [26]戴照琪,赵见营,罗辑,等.复合精油涂层对干腌火腿挥发性风味品质的影响研究[J].食品工业科技,2018,39(3):243-249,258.
- [27]王旭,张同刚,龚媛,等.响应面法优化固相微萃取-气质联用法检测低温羊肉火腿中挥发性风味物质[J].中国调味品,2015,40(10):106-111,119.
- [28]MURIEL E,ANTEQUERA T,PETRON M J,et al.Volatile compounds in Iberian dry-cured loin[J].Meat Science,2004,68(3):391-400.
- [29]MARTíN A,CORDOBA J,ARANDA E,et al.Contribution of a selected fungal population to the volatile compounds on dry-cured ham[J].International Journal of Food Microbiology,2006,110(1):8-18.