盐水鹅卤水中营养成分及挥发性特征风味物质分析Analysis of Nutritional Components and Volatile Characteristic Flavor Substances in Salted Goose Brine
李波,邵俊锋,史莹莹
摘要(Abstract):
为了比较盐水鹅新、老卤水的差异,对卤水的基本理化指标及营养成分含量进行了测定,同时运用固相顶空微萃取-气质联用技术对卤水的主体挥发性成分进行了分析。结果表明,老卤的pH及蛋白质含量显著高于新卤,脂肪和氯化钠含量差异不显著。在2种卤水中共检测出84种挥发性风味物质,其中新卤中检测出50种风味物质,主要是烃类、醛类和醇类化合物;老卤中检测出58种风味物质,主要是醛类、芳香族和烃类化合物。
关键词(KeyWords): 卤水;顶空固相微萃取-气质联用;营养成分;挥发性风味成分
基金项目(Foundation):
作者(Author): 李波,邵俊锋,史莹莹
参考文献(References):
- [1]Ramarathnam N,Rubin L J.The Flavour of Cured Meat[M].London:Blackie Academic and Professional,1994:174-198.
- [2]Derek F K,Nigel P B,Michelle M L,et al.Flavour profiling of fresh and processed fruit smoothies by instrumental and sensory analysis[J].Food Research International,2012,45(1):17-25.
- [3]Moon S Y,Cliff M A,Lichan E C.Odour-active components of simulated beef flavour analyzed by solid phase micro extraction and gas chromatography-mass spectrometry and olfactometry[J].Food Research International,2006,39(3):294-308.
- [4]Chu F L,Yaylayan V A.Model studies on the oxygeninduced formation of benzaldehyde from phenylacetaldehyde using pyrolysis GC-MS and FT-IR[J].Journal of Agricultural and Food Chemistry,2008,56(22):10697-10704.
- [5]Elnore S I,Mottram D S,Enser M,et al.Effect of the polyunsaturated fatty acid composition of beef muscle on the profile of aroma volatiles[J].J Agric Food Chem,1999,47(4):1619-1625.
- [6]Aparicio R,Luna G,Sanchez P,et al.Characterization of French and Spanish dry-cured hams:influence of the volatiles from the muscles and the subcutaneous fat quantified by SPME-GC[J].Meat Science,2005,69(4):635-45.
- [7]林翔云.香料香精辞典[M].北京:化学工业出版社,2007.
- [8]Maggi F,Papa F,Cristalli G,et al.Characterisation of the mushroom-like flavour of Melittis melissophyllum L.subsp.melissophyllum by headspace solid-phase microextraction(HS-SPME)coupled with gas chromatography(GC-FID)and gas chromatography-mass spectrometry(GC-M)[J].Food Chemistry,2010,123(4):983-992.
- [9]卢静茹,张如,吴佳,等.HS-SPME-GC-MS联用分析美国巴旦木香气成分[J].食品科学,2015,36(2):120-125.
- [10]步婷婷,徐大伦,杨文鸽,等.虾籽酱发酵工艺条件的优化及其挥发性风味成分研究[J].核农学报,2016,30(1):110-119.
- [11]刘源,徐幸莲,周光宏.南京酱牛肉风味研究初报[J].江苏农业科学,2004(5):101-104.
- [12]刘登勇,谢伟,徐幸莲.盐水鸭卤水中的挥发性物质及其风味特性分析[J].食品研究与开发,2011,32(4):118-121.