4种精油组成成分及总抗氧化活性分析研究Analysis of Composition and Total Antioxidant Activity of Four Essential Oils
陈潘,席斌,高雅琴,王芳,杨晓玲
摘要(Abstract):
实验对提取的茶树精油、薄荷精油、柚皮精油和柑橘皮精油用气相色谱-质谱联用法(GC-MS)进行成分鉴定,其中茶树精油鉴定出已知化合物48种;薄荷精油鉴定出34种;柚皮精油和柑橘皮精油各鉴定出10,11种;做总抗氧化活性分析,其活性顺序为:柑橘皮精油>柚皮精油>茶树精油>薄荷精油。萜烯类化合物含量越高,精油抗氧化活性越强,鉴定发现萜烯类化合物为4种精油的共有成分,通过对萜烯类化合物含量和总抗氧化活性的相关性进行分析,表明精油总抗氧化活性与萜烯类化合物含量呈正相关(P<0.05)。
关键词(KeyWords): 精油;茶树精油;气相色谱-质谱联用法(GC-MS);总抗氧化活性;相关性分析
基金项目(Foundation): 国家畜禽产品质量安全风险评估重大专项“畜禽产品非法定药物使用摸底排查与产品安全性评估”(GJFP20190701);; 中央级公益性科研院所基本科研业务费专项资金项目“特色畜禽肉中风味物质研究及关键控制点评估”(1610322019014)
作者(Author): 陈潘,席斌,高雅琴,王芳,杨晓玲
参考文献(References):
- [1]Sahebkar A,Iranshahi M.Biological activities of essential oils from the genus Ferula(Apiaceae)[J].Asian Biomed,2010,4(6):835-847.
- [2]何凤平,雷朝云,范建新,等.植物精油提取方法、组成成分及功能特性研究进展[J].食品工业科技,2019,40(3):307-312,320.
- [3]Hammoudi R,Dehak K,Mahammed M H,et al.Chemical composition and antioxidant activity of essential oils from Deverra scoparia Coss.and Dur.(Apiaceae)[J].Leban Sci J,2015,16(2):27-36.
- [4]Ben Marzoug H N,Romdhane M,Lebrihi A,et al.Eucalyptus oleosa essential oils:chemical composition and antimicrobial and antioxidant activities of the oils from different plant parts(stems,leaves,flowers and fruits)[J].Molecules,2011,16(2):1695-1709.
- [5]Ksouri A,Dob T,Belkebir A,et al.Chemical composition and antioxidant activity of the essential oil and the methanol extract of Algerian wild carrot Daucus carota L.ssp.carota.(L.)Thell[J]J.MaterEnvironSci,2015,6(3):784-791.
- [6]Bakkali F,Averbeck S,Averbeck D,et al.Biological effects of essential oils-a review[J].Food Chem Toxicol,2008,46(2):446-475.
- [7]Benbelad F,Khadir A,Bendahou M,et al.Composition and antimicrobial activity of Cistus munbyi essential oil:an endemic plant from Algeria[J]J.ournalofForestry Research,2017,28(6):1129-1134.
- [8]陈秀敏,方桂丽,陈敏儿,等.植物精油的抑菌作用及检测技术研究进展[J].山东化工,2017,46(10):67-69.
- [9]王会全,刘鑫,吴英祥,等.柑橘果皮精油提取工艺及成分分析研究[J].食品研究与开发,2018,39(21):92-99.
- [10]王静,李荣,姜子涛.葡萄柚薄荷精油成分的气相色谱-质谱法鉴定和抗氧化活性[J].食品科学,2013,34(15):91-94.
- [11]王芳,岳朝敏,Andreea David,等.结合GC-MS的分子蒸馏富集柚皮精油抗氧化成分的研究[J].中国粮油学报,2018(7):65-71.
- [12]Bárbara Teixeira,António Marques,Cristina Ramos,et al.Chemical composition and antibacterial and antioxidant properties of commercial essential oils[J].Industrial Crops and Products,2013,43(1):587-595.
- [13]Massada Y.Analysis of essential oil by gas chromatography and spectrometry[J].John Wiley&Sons Inc.in New York,1976:95-221.
- [14]Adams R P.Identification of essential oil components by gas chromatography/mass spectroscopy[J].Journal of the American Society for Mass Spectrometry,1997.
- [15]贾德翠,涂洪强,王仁才,等.椪柑果皮精油成分的GC-MS分析[J].湖南农业科学,2009(2):105-107.
- [16]朱凤妮,卢剑青,陈金印,等.江西省6种宽皮柑橘类黄酮及挥发油成分的研究[J].果树学报,2017,34(9):1106-1116.
- [17]冯璐璐,毛运芝,冉慧,等.6种宽皮柑橘果皮精油GC-MS鉴定与组分差异分析[J].果树学报,2018,35(4):412-422.
- [18]石金娥,杨波,王莹,等.顶空-气相色谱/质谱法测定互叶白千层茶树精油中的挥发性成分[J].食品安全质量检测学报,2019,10(6):1530-1533.
- [19]GB/T 26514-2011,互叶白千层(精)油,松油烯-4-醇型[茶树(精)油][S].
- [20]Hammer K A,Carson C F,Riley T V,et al.A review of the toxicity of Melaleuca alternifolia(tea tree)oil[J].Food and Chemical Toxicology,2006,44:616-625.
- [21]王少铭,侯颖辉,刘济明,等.贵州不同地区品种间留兰香薄荷精油成分比较[J].中国调味品,2019,44(2):141-145.
- [22]冯堃,秦昭,王文蜀,等.5种柚皮精油成分及油脂抗氧化和抑菌活性[J].食品科技,2018,43(11):255-261.
- [23]黄娜娜.柑橘精油抗氧化特性及对皮肤细胞氧化损伤的保护作用研究[D].武汉:华中农业大学,2016.
- [24]李勇慧,耿惠敏,李双双.四种柑橘类果皮精油成分分析[J].现代食技,2019,35(4):264-272.
- [25]周立华,牟德华,李艳.7种小浆果香气物质的GC-MS检测与主成分分析[J].食品科学,2017,38(2):184-190.
- [26]吕海鹏,林智,张悦,等.不同等级普洱茶的化学成分及抗氧化活性比较[J].茶叶科学,2013,33(4):386-395.