二乙胺滴定法测定辣根及芥末制品中异硫氰酸酯含量的研究Titrimetric method for quantitative determination of the isothiocyanates with diethy amine
张清峰,姜子涛,董峰光,李荣
摘要(Abstract):
本文报道了测定辣根及芥末制品中异硫氰酸酯含量的一种新方法--二乙胺滴定法。异硫氰酸酯与二乙胺在丙酮溶液中发生均相反应,生成相应的硫脲,过量的二乙胺用标准盐酸滴定,从而计算出异硫氰酸酯的含量。通过与哌啶法、吗啉法的对比实验,表明该法准确可靠、简便易行。
关键词(KeyWords): 异硫氰酸酯;二乙胺;辣根;芥末
基金项目(Foundation): 天津市自然科学基金(043604511) 天津市高校科技发展基金(20030905)资助课题
作者(Author): 张清峰,姜子涛,董峰光,李荣
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