磁性壳聚糖糖用澄清剂的制备及结构表征Preparation and Structural Characterization of Magnetic Chitosan as Sugarcane Juice Clarifying Agent
范松林,张佳欣,宋小荣,梁欣泉
摘要(Abstract):
以壳聚糖(CTS)为原料,通过化学共沉淀一步法制备出磁性壳聚糖(MCTS),以取代糖业传统澄清剂SO_2。用该产物澄清糖厂甘蔗汁,并以清汁脱色率和纯度差为评价指标,通过单因素实验与正交实验优化制备工艺条件,利用扫描电镜(SEM)、傅里叶红外变换光谱仪(FT-IR)、X射线衍射仪(XRD)和振动样品磁强计(VSM)对其进行结构表征及性能分析。实验结果表明:在NaOH质量分数为20%、戊二醛质量分数为1%、交联时间为2h及壳聚糖的添加量为1.25g的条件下,所制备出的磁性壳聚糖的澄清效果最好,脱色率可达55.55%,纯度差可达2.80%。通过与糖厂传统澄清剂SO_2的澄清效果进行比较,认为可以用磁性壳聚糖取代SO_2应用于甘蔗汁的澄清过程。
关键词(KeyWords): 磁性壳聚糖;蔗汁;脱色率;纯度差
基金项目(Foundation): 糖蜜酒精精馏过程节能技术开发及应用示范(AE120094);广西区特色本科专业建设项目——食品科学与工程(制糖工程)
作者(Author): 范松林,张佳欣,宋小荣,梁欣泉
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