王苑力,杨剀舟,魏征,栾霞

• 1:国家粮食和物资储备局科学研究院
• 2:福汇生物科技(广东)有限公司

摘要(Abstract)：

以云南罗平小黄姜为研究对象，研究了超声-溶剂浸提联合提取姜油树脂的新工艺，通过响应面法对提取工艺进行优化，并利用固相微萃取(solid-phase microextraction, SPME)和气相色谱-质谱联用技术(gas chromatography-mass spectrometry, GC-MS)探究此方法下得到的姜油树脂的香气组成及关键呈香成分。结果表明，以石油醚为溶剂，姜油树脂的最佳提取条件为料液比1∶8、超声功率160 W、超声时间30 min、提取温度65℃、提取时间5.8 h,此条件下得到产品中6-姜酚浓度最高，为106.77 mg/g;产品中共鉴定出77种挥发性成分，其中以荜澄茄油宁烯、花侧柏烯、反式-α-没药烯等化合物的相对含量较高，结合香气活性值(odor activity value, OAV)分析表明，对姜油树脂具有香气贡献的特征香气成分共36种，贡献最大的为醇类化合物桉树醇，其OAV为1.77×10~6,呈桉树樟脑味；其次为呈薄荷味、松节油味的β-水芹烯和呈辣香味的月桂烯。该研究结果可为姜油树脂的提取工艺提供新的思路，同时为罗平小黄姜姜油树脂的呈香特征、香气形成机制、产品品质改善等提供参考依据，利于带动当地产业发展。

关键词(KeyWords)： 姜油树脂;响应面;挥发性化合物;香气活性值;特征香气成分

Abstract:

Keywords:

基金项目(Foundation): 国家专利成果转化运用项目(H19036)

作者(Author): 王苑力,杨剀舟,魏征,栾霞

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