响应面优化提取灰绿碱蓬多糖及脱色工艺研究Study on Optimization of Extraction and Decolorization Process of Polysaccharides fromSuaeda glauca Bunge.by Response Surface Method
付建鑫,邵家威,方奕珊,张桂香
摘要(Abstract):
应用响应面法在单因素试验基础上对灰绿碱蓬多糖提取条件进行优化,测定了灰绿碱蓬根、茎、叶的基本营养物质成分,并对多糖脱色工艺进行探究。乙醇体积分数65%、提取时间72min、超声功率438 W,提取温度85℃为最佳提取参数,此时碱蓬多糖提取得率达到2.19%±0.13%。选择HZ-800大孔树脂作为碱蓬多糖的脱色方式,添加量为1.8%,脱色率为95.51%,多糖保留率为79.62%,此时脱色效果和多糖保留率最好。
关键词(KeyWords): 灰绿碱蓬;响应面;脱色;得率
基金项目(Foundation): 国家自然科学基金(21705084);; 山东省自然科学基金(ZR2017BB074);; 山东省科技重大专项(2015ZDJJQ07003)
作者(Author): 付建鑫,邵家威,方奕珊,张桂香
参考文献(References):
- [1]李敏,刘帅帅,徐飞.黄河三角洲芦苇-碱蓬群落结构和功能对3种人为干扰的响应[J].湿地科学,2017,15(1):92-98.
- [2]王恒禹,刘玥,姜猛,等.多糖在食品工业中的应用现状[J].食品科学,2013,34(21):431-438.
- [3]Yang Mengna,Sun Hongjuan,Peng Tongjiang,et al.Structural alteration of montmorillonite by acid activation and its effect on the decolorization of rapeseed oil[J].JOM,2019,71(10):3665-3673.
- [4]Yin Qiang,Zhou Gang,Peng Can,et al.The first fungal laccase with an alkaline pH optimum obtained by directed evolution and its application in indigo dye decolorization[J].AMB Express,2019,9(1):878-880.
- [5]Mahsa Rashidi,S Maryam Sajjadi,Hassan Zavvar Mousavi.Kinetic analysis of azo dye decolorization during their acidbase equilibria:photocatalytic degradation of tartrazine and sunset yellow[J].Reaction Kinetics,Mechanisms and Catalysis,2019,128(1):1654-1655.
- [6]李美玲,王卓琳,黎庆涛,等.焦糖色素及其研究进展[J].中国调味品,2019,44(9):183-187.
- [7]徐景峰.皂土处理及其对染料脱色和重金属脱除的效果研究[J].广州化工,2018,46(11):52-54,67.
- [8]Jiang Li,Li Hao,Wang Yanan,et al.Characterization of carbon deposits on coked lithium phosphate catalysts for the rearrangement of propylene oxide[J].Catalysis Communications,2015,64:22-26.
- [9]陆敏,马海乐,朱莉萍,等.D301-G大孔树脂吸附菊芋多糖色素机理探究[J].食品工业科技,2019,40(16):58-63,70.
- [10]王娣,李雨晴,程柏,等.响应面优化百里香多糖提取工艺及其抗氧化作用[J].中国调味品,2019,44(8):105-109.
- [11]岳珍珍,王静,方利英,等.大孔吸附树脂对刺梨果汁单宁脱除及其色泽的影响[J].食品科学,2016,37(17):109-114.
- [12]陈琛,戴士博.铁粉和过氧化氢不同比例对偶氮脱色效果的影响[J].水科学与工程技术,2019(2):59-62.
- [13]张从聪,张琳萍,徐红,等.配合物CO3(BTB)2(H2O)5(DMF)9的合成及其催化染料废水脱色性能研究[J].广东化工,2017,44(2):10-12.
- [14]张晓旭,周锡钦,胡思齐,等.超声辅助有机溶剂法提取青花椒色素的工艺研究[J].中国调味品,2019,44(8):185-188.
- [15]张红,万文婷,岳红霞,等.乐陵金丝小枣枣皮色素提取工艺的优化[J].中国调味品,2019,44(5):180-183.
- [16]李昌文,张丽华,纵伟.黑米色素的提取工艺及生物活性研究进展[J].中国调味品,2019,44(7):168-170,175.
- [17]Cui Jie,Gu Xin,Wang Fengjun,et al.Purification and structural characterization of anα-glucosidase inhibitory polysaccharide from apricot(Armeniaca sibirica L.Lam.)pulp[J].Carbohydrate Polymers,2015,121:309-314.
- [18]Fan Yina,Wu Xiangyang,Zhang Min,et al.Physical characteristics and antioxidant effect of polysaccharides extracted by boiling water and enzymolysis from Grifola frondosa[J].International Journal of Biological Macromolecules,2011,48(5):798-803.
- [19]刘力萍,吴天祥,张宗启.灰树花胞外多糖不同脱色方法的研究[J].食品科技,2018,43(11):196-201.
- [20]付玲,张帅,吕林霞,等.NO在Ir(111)表面吸附与解离的第一性原理研究[J].原子与分子物理学报,2018,35(3):395-400.